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CM2142 Expt2.5 and 2.9
CM2142 Expt2.5 and 2.9
Expt 2.5 - Identification of Synthetic Food colors by Thin Layer Chromatography
Expt 2.9 - Water Analysis






See also: CM2142 Expt 2.5 and Expt 2.9
Expt 2.5 - Identification of Synthetic Food colors by Thin Layer Chromatography
Expt 2.9 - Water Analysis
See also: CM2142 Expt 2.5 and Expt 2.9
CM2121 Expt 2
CM2121 Expt 2
a) Protection of 1-Phenylethanol by 3,4-Dihydro-2H-pyran
b) Purification of 2-(1-Phenylethoxy)-tetrahydro-2H-pyran by Flash Column Chromatography


Starting material (1-Phenylethanol)

1-Phenylethanol with 3,4-Dihydro-2H-pyran and anhydrous ether in cold bath with calcium chloride guard tube.

Toluenesulfonic acid monohydrate added and stirring with magnetic stirrer.

TLC with hexane:ethyl acetate (4:1) solvent system to confirm convertion

Washing of organic layer with saturated sodium bicarbonate solution followed by saturated sodium chloride solution.

Remove the solvents using the rotary evaporator


Flash Column Chromatography

See also: CM2121 Expt 2
a) Protection of 1-Phenylethanol by 3,4-Dihydro-2H-pyran
b) Purification of 2-(1-Phenylethoxy)-tetrahydro-2H-pyran by Flash Column Chromatography
Starting material (1-Phenylethanol)
1-Phenylethanol with 3,4-Dihydro-2H-pyran and anhydrous ether in cold bath with calcium chloride guard tube.
Toluenesulfonic acid monohydrate added and stirring with magnetic stirrer.
TLC with hexane:ethyl acetate (4:1) solvent system to confirm convertion
Washing of organic layer with saturated sodium bicarbonate solution followed by saturated sodium chloride solution.
Remove the solvents using the rotary evaporator
Flash Column Chromatography
See also: CM2121 Expt 2
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